创见|实干|卓越
与光同程,做民族仪器企业

光解水water-splitting reaction

Labsolar-6A 全玻璃自动在线微量气体分析系统

Labsolar-6a All-glass automatic on-line trace gas analysis system

产品中心:光解水品牌:泊菲莱浏览量:60581
Labsolar-6A 全玻璃自动在线微量气体分析系统集成控制程序,操作简单方便,强大的兼容性,可通过更换不同的反应器实现光催化、光热催化、电催化、PEC光电化学等反应的微量气体检测。
  • 产品介绍
  • 应用领域
  • 文献
  • 技术维护

关键特征

● 玻璃阀+自动执行器,实现气密性与效率兼顾的目标;

● 高效气体循环,既有效促进反应与催化剂之间的传质作用,又有效避免因产物分子的重吸附作用引发的副反应和逆反应,准确呈现催化剂的本征活性;

● 气体快速混合,气体混匀时间<10 min,确保产物检测的准确性;

● 集成控制程序,操作简单方便,准确性达科学级水准;

● 强大的兼容性,可通过更换不同的反应器实现光催化、光热催化、电催化、PEC光电化学等反应的微量气体检测。

 

应用领域

▲特别适用   ●较为适用  ○可以使用

▲ 光催化/光电催化分解水制氢/氧

▲ 光催化/光电催化全分解水

▲ 光催化/光电催化CO2还原

▲ 光催化量子效率测量

▲ 光热催化(负压常压体系)

▲ 电催化HER、OER、CO2RR

 

可搭配多种反应器拓展应用

 

气体循环参数

气体混匀时间:H2、O2、CH4、CO混匀时间<10 min;

标准曲线线性:H2含量为100 μL~10 mL范围时,R2>0.9995;

重复性:同一浓度连续四次进样,RSD<3%;

排气量 :6 mL/次,负压至常压均能提供优异的循环驱动力;

无源磁驱柱塞泵:管路中无电线接入,无氢爆风险,不产生电解水析氢干扰;具有单向阀结构,可实现所有管路的单向循环;

取样方式:定量环位于多通玻璃取样阀,非色谱取样;

循环管路:最窄管路为内径为3 mm,非小口径色谱管路,气体阻力小

外观结构参数

反应器:可适配光催化反应器、光电催化、光热催化反应器;可根据实际实验需求定制;

整机尺寸/mm:490 (L)×520 (W)×740 (H)

金属防护箱体:对辐射可能的气体泄漏有一定防护作用

光防护罩:便携式光防护罩,可有效防止光污染

 

系统管路参数

绝压真空度:≤1.5 kPa

使用压力范围:0 kPa~常压

阀门数量:7

管路体积:65 mL,系统富集能力强

管路材质:高硼硅玻璃,高化学惰性,无吸附

阀门工艺:高硼硅玻璃材质,阀塞与阀套采用对磨精磨工艺

真空脂:进口道康宁真空脂,耐化学品的侵蚀,低蒸汽压力,低挥发性,工作温度:-40℃~200℃

定量环:0.6 mL、2 mL可选,系统灵敏度可调

储气瓶:150 mL,适用系统扩容和反应气如二氧化碳的存储

管路控温:循环管路及进样管路均可进行控温,最高可控200℃ ;10段程序控温,控温精度±0.1℃;

冷凝管(球形/蛇形):冷凝充分,避免水蒸气进入气相色谱仪和真空泵

冷阱(选配):分离低沸点组分,延长真空泵使用寿命,提高系统真空度

控制单元参数

软件模块:32位控制软件和4.5寸TFF彩色触摸屏 ;内置仪器方法用于控制玻璃阀动作、气相色谱仪及真空泵启停,操作简单;自动控制模式下,可实时显示阀门位置,具有安全防护预警功能;传感器自动提示更换真空脂;具有二级加密调试程序,用于设备调试、内部方法设定及资深用户灵活使用;实时显示系统内部反应压力、环境温度等参数;

自动取样阀:高硼硅玻璃材质,内置定量环 ;多通复合取样阀,减少系统循环体积 ;支持手动、自动、半自动操作模式;

真空泵:系统控制软件自动控制启停,间歇式工作,噪音小; 含单向电磁阀,可防止泵油倒吸;

检测参数

检测范围:H2、O2、CH4、CO等多种微量气体;

检出限/μmol:H2:0.05;O2:0.1;CH4/CO:0.0005。

代表文献

华东理工大学李春忠团队引用Labsolar-6A光催化反应系统

青岛科技大学李镇江团队引用Labsolar-6A光催化反应系统.png

陕西师范大学蒋加兴团队引用Labsolar-6A光催化反应系统

陕西师范大学刘生忠团队引用Labsolar-6A光催化反应系统

应化所王颖团队引用Labsolar-6A光催化反应系统

深圳大学团队引用Labsolar-6A全玻璃微量气体分析系统.png

  • 膜光催化
  • 光降解气体污染物
  • 光热催化(负压常压体系)
  • PEC光电化学
  • 光催化量子效率测量
  • 电化学
  • 光催化二氧化碳还原
  • 光催化全分解水
  • 光催化分解水制氢/氧
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